iphepha_ibhena

130878-68-1 Fmoc-L-Val-Osu

130878-68-1 Fmoc-L-Val-Osu

Inkcazelo emfutshane:

Imbonakalo Umgubo omhlophe ukuya kumhlophe
MF I-C24H24N2O6
MW 436.46
Ubunyulu 95+


Iinkcukacha zeMveliso

Imeko yezothutho
Inokuthuthwa kubushushu obuqhelekileyo.

Cebisa indlela yokuthumela ngenqanawa
ngomoya, ngomhlaba okanye ngolwandle

Imeko yokugcina:
I-2-8 ° C, kufuneka igcinwe kwindawo evaliweyo, ebandayo kwaye engenalanga.

beka ubomi kwishelufa
malunga neminyaka emi-2

Ubuncinci uMyalelo weQty:
1kg (uthethathethwano)

Isiqinisekiso:COA, indawo yokunyibilika, iSpecificRotation [α]D20  Siza kuthumela nayiphi na idatha oyifunayo.Kodwa kwiimveliso ezenziwe ngokwezifiso, sithumela idatha entsha emva kokuba iphumile.
Ngokuqinisekileyo, unokubona idatha ngaphambili njengereferensi.

I-D-Ls(tfa)-NCA (2)

Izithethantonye

CarbaMicacid, [1-[[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl]-2-Methylpropyl]-,9H-fluoren-9-ylMethylester,(S)-;

L-Valine,N-[(9H-fluoren-9-ylmethoxy)carbonyl]-,2,5-dioxo-1-pyrrolidinylester;

N-Fmoc-L-valineN-succinimidylester;

I-Fmoc-L-valineN-hydroxysuccinimideester≥99%(HPLC);

FMOC-L-VALINEN-HYDROXYSUCCINIMIDEESTER;

FMOC-VAL-OSU;

FMOC-VALINE-OSU;

NALPHA-9-Fluorenylmethoxycarbonyl-L-valineN-hydroxysuccinimideester

Ukupakishwa kwangaphakathi

Zihlala zisetyenziselwa ukupakisha umgubo.Kuxhomekeke kwiimfuno zabathengi.Ke ngoko, sixelele ngemfuno yakho phambi kokupakisha ukuba unezicelo ezizodwa.

Ukupakisha kwangaphakathi 2
Ukupakisha kwangaphakathi 1
Ukupakisha kwangaphakathi 3

ukupakisha kwangaphandle

I-1kg ukuya kwi-25kg Ukupakisha kwangaphandle kunzima.Kwaye kunzima ukusika kunye nomonakalo.Inokukhusela iimveliso zakho ngokugqibeleleyo.

Ukupakisha kwangaphandle 3
Ukupakisha kwangaphandle 2
Ukupakisha kwangaphandle 1

Usetyenziso

I-Ester yenziwe kwi-esterization reaction ye-asidi ye-inorganic okanye i-asidi ephilayo okanye utywala.Utywala okanye i-phenol okanye i-anhydride ene-acidic, i-alcohol kunye ne-ethylene, i-acidic yamahhala kunye ne-fatty nitrogen derivatives nayo inokuvelisa i-ester.I-hydrogen kwi-alpha-carbon kwii-molecule ze-ester ilahlekelwa utywala be-molecular kunye nenye i-molecular ester phantsi kweemeko ze-alkaline ukuvelisa i-β-keto ester, ebizwa ngokuba yi-ester contraction reaction.Ngokomzekelo, i-acetyl acetate yenziwe ukuvelisa i-acetyl ethyl acetate.Le mpendulo ibaluleke kakhulu kwi-organic synthesis.

Igama le-ester livela kwigama elihambelanayo le-carboxylic acid kunye notywala okanye i-phenol, njenge "asidi ethile kunye ne-ester ethile".Ii-esters zesangqa zibizwa ngokuba yilactone (lactone).Iimpawu zeekhemikhali ze-ester zifana ne-amyl niche anhydride, ejongene ne-hydrolysis, utywala kunye ne-ammonia reaction.I-ester yomgangatho ophantsi inevumba elimnandi kunye nolwelo oluguquguqukayo olungenambala, kwaye i-ester ephezulu iqinile.I-Estes zizinyibilikisi ezibalulekileyo kunye nemathiriyeli ekrwada yokwenziwa, kwaye ezinye ii-esters ziziyobisi ngokwazo.Ngokohlobo lwe-asidi, i-ester inokohlulwa ibe yi-ester ye-asidi ye-inorganic kunye ne-organic acid ester.I-Etate, i-ethyl acetate yi-ester enamafutha, i-acetate yi-ester enevumba elimnandi, kunye ne-namanonate yi-cyclic ester.

iimveliso ezinxulumene

Cbz-L-Val-Osu Cbz-D-Val-Osu I-Boc-L-Val-OSU L-Val-OH
HD-Val-OH Boc-L-Val-OH Boc-D-Val-OH Boc-L-Val-OL
Fmoc-L-Val-OH Fmoc-D-Val-OH Fmoc-D-Val-Osu Boc-Val-Val-OH

Kutheni Khetha Thina

1. Malunga ne-MOQ: Sinokuyilungisa ngokwemfuno yakho.
2. Malunga nesampuli: Isampuli idinga umrhumo wesampuli, onokuthi ube yimpahla yokuqokelela okanye unokuhlawula kuthi kwangaphambili.
3. Iworkshop yokubunjwa, inokwenziwa ngokwezifiso ngokwenani leemodeli.
4. Sinikezela ngeyona nkonzo ibalaseleyo.Iqela lokuthengisa elinamava sele lisebenzela wena.
5. Malunga notshintshiselwano: Nceda uthumele i-imeyile okanye uxoxe nam ngokufanelekileyo.


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