INCWADANA YEENDABA
Ngemibuzo malunga neemveliso zethu okanye uluhlu lwamaxabiso, nceda ushiye i-imeyile yakho kuthi kwaye siya kuqhagamshelana phakathi kweeyure ezingama-24.
BUZA NGOKUImeko yezothutho&ecetyiswayo indlela yokuthumela ngenqanawa:
ngomoya, ngolwandle okanye nge-express
Imeko yokugcina:
2-8°C
Ubuncinci boMyinge woMyalelo:
Uthethathethwano
Isiqinisekiso:
COA, HPLC, GC, HNMR, Assay, Water Content(KF), TLC iyafumaneka
Boc-3-(Fmoc-amino)-L-alanine,Nα-Boc-Nβ-Fmoc-L-2,3-diaminopropionicacid;
I-NALPHA-tert-Butoxycarbonyl-NB-9-fluorenylmethoxycarbonyl-L-2,3-diaminopropi;
N-.ALPHA.-BOC-N-.BETA.-FMOC-L-2,3-DIAMIOPROPIONICACID;
I-N-Boc-N-Fmoc- (S) -2,3-diaminopropionicacid;
I-N-α-Boc-N-β-Fmoc-L-2,3-diamiopropionicacid;
(S) -2,3-Diaminopropanoicacid,N2-BOC,N3-FMOCekhuselweyo;
3-[(9H-Fluoren-9-ylmethoxycarbonyl)amino]-L-alanine,N-BOCKhuselweyo;
Boc-Dapa(FMoc)-OH
Ngokuqhelekileyo zisetyenziselwa ukupakisha umgubo.Yaye anokuthintela ukukhanya kwelanga namanzi ukuba angabi mabi.
Ibhokisi elukhuni inokukhusela iimveliso zakho ekuqhekekeni kwaye zibe manzi.
I-amino acids ekhusela kabini ikakhulu ibandakanya i-D-lys-OH equlathe amaqela e-amino ecala kunye nekhonkco elisecaleni eliqulathe ikhonkco.pukujikelezwa kwe-L-Rag-OH.Kwiqela le-AA-amin, isicwangciso sokukhusela i-FMOC sisamkelwa, kwaye umalume wesibini we-carbonate-carbonate usetyenziswa kwi-chain chain.I-Tibon ifakwe kwiqela lemibhobho ye-oksijeni ukuze ikhusele iFu Fu 5 ~ Sulfidal ukukhusela.Ngenxa yokuba kukho amanyathelo amaninzi okudibanisa ezi zimbini ze-amino acids, impendulo ephambili kwimpendulo ephambilisI-teps yenza imifuniselo yokwandisa into enye.Ukukhuselwa kwe-D-LYS-OH ikakhulu kuqwalaselwa ixesha elichaphazela isizukulwana sobheduiubushushu, kunye nexesha lokukhupha ubhedu.Ukukhuselwa kwe-L-Rag-OH ikakhulu kuqwalaselwa ukulungiswa kwe-Z-RG-OH. Ngelo xesha, ubushushu be-ZL-Rag (PBF) -OH ring yetyuwa ye-ammonia, kunye nomlinganiselo we-catalyst xa i-hydrogen ihlanganiswe ne-Z,tUxinzelelo lwakhe, ubushushu kunye nexesha lokuphendula lifumene imveliso elungileyo ngokusebenzisa imifuniselo yokuphucula.
Ngexesha lenkqubo yokusabela, inkqubo yokujonga i-TL.C yokufumanisa ithathwa ngokuyintloko, kwaye iimeko ze-crystallization zemveliso ziphuculwe.
Ukucoceka kwemveliso kulinganiswa ne-high-efficiency liquid chromatography, kwaye ukucoceka kwemveliso kufikelele ngaphezu kwe-95.0%.Ukongeza kwiimpawu eziqhelekileyo zomzimba eziqhelekileyo, kwakhonaiukuquka infrared spectrum, mass spectrum okanye hydrogen spectrum.
Boc-D-Dap(Boc).DCHA | Boc-Dap(Boc)-OH.DCHA | I-Boc-D-Dap(Fmoc)-OH | Boc-Dap(Cbz)-OH |
Boc-D-Dap(Cbz)-OH | Fmoc-L-Dap(Fmoc)-OH | Fmoc-L-Dap(Cbz)-OH | Fmoc-D-Dap(cbz) |
Cbz-D-Dap(BOC)-OH | Cbz-L-Dap(Fmoc)-OH |
1. Inkonzo yeR&D iyafumaneka
2. Umvelisi oqinisekisiweyo we-ISO, isiqinisekiso somgangatho
I-3.Ikhosi epheleleyo yenkonzo yokulandelela ngexesha lemveliso
4.Ixabiso eliphezulu elisebenzayo
5.Amaxwebhu esiqinisekiso somgangatho anikwe ngokwesicelo somthengi
I-6.Inkonzo enkulu emva kokuthengisa, ukugcina ubudlelwane obusondeleyo kunye nomthengi
I-7.Isixhobo esipheleleyo sokunceda ukunciphisa iindleko zokuthumela ngenqanawa
I-8.Isampuli yamahhala enikezelwa ukujonga umgangatho ngaphambi kwayo nayiphi na intlawulo
9.Ixesha lentlawulo ekuxoxwe ngalo
Abathengi be-10.Assit bajongana nemicimbi yaseTshayina