China 75932-02-4 N-α,N-ε-di-Fmoc-D-lysine Umvelisi kunye neFactory |Jiayinglai

75932-02-4 N-α,N-ε-di-Fmoc-D-lysine

Inkcazelo emfutshane:

Imbonakalo	Umgubo omhlophe ukuya kumhlophe
MF	I-C36H34N2O6
MW	590.66
Ubunyulu	98+

Thumela i-imeyile kuthi

Iinkcukacha zeMveliso

Imeko yezothutho&ecetyiswayo indlela yokuthumela ngenqanawa:
ngomoya, ngolwandle okanye nge-express

Imeko yokugcina:
2-8°C

Ubuncinci boMyinge woMyalelo:
Uthethathethwano

Isiqinisekiso:
COA, HPLC, GC, HNMR, Assay, Water Content(KF), TLC iyafumaneka

Izithethantonye

Na,Ne-di-Fmoc-D-lysine;

N-.ALPHA.,N-.EPSILON.-DI-FMOC-D-LYSINE;

(R) -1,13-di(9H-fluoren-9-yl)-3,11-dioxo-2,12-dioxa-4,10-diazatridecane-5-carboxylicacid;

D-Lysine,N2,N6-bis[(9H-fluoren-9-ylMethoxy)carbonyl]-;

I-FMoc-D-Lys(FMoc)-OHN-α,N-ε-di-FMoc-D-lysine;

N2,N6-Bis-FMoc-D-lysine;

N2,N6-Bis[(9H-fluoren-9-ylMethoxy)carbonyl]lysine

Ukupakishwa kwangaphakathi

Ngokuqhelekileyo zisetyenziselwa ukupakisha umgubo.Yaye anokuthintela ukukhanya kwelanga namanzi ukuba angabi mabi.

ukupakisha kwangaphandle

Ibhokisi elukhuni inokukhusela iimveliso zakho ekuqhekekeni kwaye zibe manzi.

Usetyenziso

I-amino acids ekhusela kabini ikakhulu ibandakanya i-D-lys-OH equlathe amaqela e-amino ecala kunye nekhonkco elisecaleni eliqulathe ikhonkco.pukujikelezwa kwe-L-Rag-OH.Kwiqela le-AA-amin, isicwangciso sokukhusela i-FMOC sisamkelwa, kwaye umalume wesibini we-carbonate-carbonate usetyenziswa kwi-chain chain.I-Tibon ifakwe kwiqela lemibhobho ye-oksijeni ukuze ikhusele iFu Fu 5 ~ Sulfidal ukukhusela.Ngenxa yokuba kukho amanyathelo amaninzi okudibanisa ezi zimbini ze-amino acids, impendulo ephambili kwimpendulo ephambilisI-teps yenza imifuniselo yokwandisa into enye.Ukukhuselwa kwe-D-LYS-OH ikakhulu kuqwalaselwa ixesha elichaphazela isizukulwana sobheduiubushushu, kunye nexesha lokukhupha ubhedu.Ukukhuselwa kwe-L-Rag-OH ikakhulu kuqwalaselwa ukulungiswa kwe-Z-RG-OH. Ngelo xesha, ubushushu be-ZL-Rag (PBF) -OH ring yetyuwa ye-ammonia, kunye nomlinganiselo we-catalyst xa i-hydrogen ihlanganiswe ne-Z,

Uxinzelelo, ubushushu kunye nexesha lokuphendula lifumene imveliso elungileyo ngokusebenzisa imifuniselo yokuphucula.

Ngexesha lenkqubo yokusabela, inkqubo yokujonga i-TL.C yokufumanisa ithathwa ngokuyintloko, kwaye iimeko ze-crystallization zemveliso ziphuculwe.

Ukucoceka kwemveliso kulinganiswa ne-high-efficiency liquid chromatography, kwaye ukucoceka kwemveliso kufikelele ngaphezu kwe-95.0%.Ukongeza kwiimpawu eziqhelekileyo zomzimba eziqhelekileyo, kwakhonaiukuquka infrared spectrum, mass spectrum okanye hydrogen spectrum.

iimveliso ezinxulumene

L-Ls(Boc)	Lys(Fmoc)-OH	L-Lys(Cbz)-OH	D-Ls(Fmoc) .HCl
Lys(Fmoc).HCl	Boc-Lys(Boc)-OH	Boc-L-Lys(Boc)-OH·DCHA	Boc-D-Lys(Boc)-OH
Boc-L-Lys(Fmoc)-OH	Fmoc-L-Lys(tfa)-OH	I-Fmoc-L-Ls(DDC)	Fmoc-L-Lys(Cbz)
I-Fmoc-L-Lys(AC)	Fmoc-L-Lys(Fmoc)-OH	Fmoc-D-Lys(Boc)-OH	Fmoc-L-Lys(Boc)-OH
Cbz-L-Lys(Fmoc)-OH	Z-DL-Lys(cbz)-OH
Fmoc-Gly-Ol	Gly-Gly-Leu	H-Gly-Obzl.Tos	Boc-Trp-Gly
Fmoc-Gly-OH	Gly-Gly-Gly	Gly-Obzl	Fmoc-L-Thr(tBu)-Gly-OH
Fmoc-Gly-Val-OH	Ala-gly	Gly-Obzl.hcl	I-Met-Gly.HCl
Fmoc-Gly-Gly-OH	Ala-Gly-Ome.hcl	Tos-Gly-Ome	H-Met-Gly-OH
Fmoc-Gly-Gly-Gly-OH	Boc-Ala-Gly-OH	H-Gly-Oet.HCl	Cbz-D-Arg-Gly-OH
Fmoc-Gly-Gly-Gly-Gly-OH	Fmoc-Ala-gly-OH	Gly.HCL	Boc-Wakhe(Trt)-Gly-OH
H-Gly-NH2.HCl	Boc-Gly-OL

Ukongama

1. Inkonzo yeR&D iyafumaneka
2. Umvelisi oqinisekisiweyo we-ISO, isiqinisekiso somgangatho
I-3.Ikhosi epheleleyo yenkonzo yokulandelela ngexesha lemveliso
4.Ixabiso eliphezulu elisebenzayo
5.Amaxwebhu esiqinisekiso somgangatho anikwe ngokwesicelo somthengi
I-6.Inkonzo enkulu emva kokuthengisa, ukugcina ubudlelwane obusondeleyo kunye nomthengi
I-7.Isixhobo esipheleleyo sokunceda ukunciphisa iindleko zokuthumela ngenqanawa
I-8.Isampuli yamahhala enikezelwa ukujonga umgangatho ngaphambi kwayo nayiphi na intlawulo
9.Ixesha lentlawulo ekuxoxwe ngalo
Abathengi be-10.Assit bajongana nemicimbi yaseTshayina